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doi: 10.1007/s43450-021-00130-z 127

99.79% Batch 1102 Tirzepatide 30 mg Method HPLC + MS Analysed 25 Nov 2025 Verify key MLMITMZ31PEL 99.31% Batch 1024 Retatrutide 30 mg Method HPLC + MS Analysed 25 Nov 2025 Verify key PKW8B1K4Q4YR 95.54% Batch blue HGH 10 IU (rHGH) Method HPLC + MS Analysed 22 Dec 2025 Verify key 8IYC2342HSVD 99.65% Batch LOT#0709 GHK-Cu 100 mg Method HPLC + MS Analysed 23 Sept 2025 Verify key X1D18PG3PV1G 99.77% Batch LOT#2708 DSIP 5 mg Method HPLC + MS Analysed 23 Sept 2025 Verify key QR37GZ45HKRI 99.93% Batch #0816 TB-500 Fragment 10 mg Method HPLC + MS Analysed 2 Sept 2025 Verify key ZA3G75VMCBHC 99.86% Batch aura003 Retatrutide 15 mg Method HPLC + MS Analysed 10 Jul 2025 Verify key FPRAJRDMSPN7 7647 IU Batch aura004 HCG 5000 IU Method Immunoassay Analysed 28 Jul 2025 Verify key 5VYZCFUKAQ8A BPC-157 6.58 mg TB-500 7.16 mg Batch 50-502 BPC-157 5 mg / TB-500 Blend Method HPLC + MS Analysed 27 Jun 2025 Verify key G4ENR7RMSWEW 99.11% Batch 50-502 AOD-9604 5 mg Method HPLC + MS Analysed 17 Jun 2025 Verify key 86RA5BXNNHLZ 10.61 mg 10.33 mg (99.663% / 99.760%) Batch 1102 Tirzepatide 10 mg Method HPLC + MS Analysed 25 Nov 2025 Verify key V4W6RGXRMHD5 5.12 mg 5.36 mg (99.884% / 99.907%) Batch 0907 Semaglutide 5 mg Method HPLC + MS Analysed 14 Nov 2025 Verify key K7NH5ZWG4QCD 9.88 mg 10.35 mg (99.502% / 99.529%) Batch yellow Survodutide 10 mg Method HPLC + MS Analysed 22 Dec 2025 Verify key TH5L345AWNXM 99.97% Batch aura004 Tirzepatide 40 mg (T40) Method HPLC + MS Analysed 28 Jul 2025 Verify key 2NHJ57K8PDBE 99.34% Batch aura004 Tesamorelin 10 mg Method HPLC + MS Analysed 28 Jul 2025 Verify key AVT44Q9MSLYS 99.64% Batch aura004 Melanotan I 10 mg Method HPLC + MS Analysed 28 Jul 2025 Verify key N42M2WYDK4SE 99.85% Batch aura003 Tirzepatide 10 mg Method HPLC + MS Analysed 10 Jul 2025 Verify key 8AGXDPSDJA45 99.87% Batch #0816 TB-500 Fragment 5 mg Method HPLC + MS Analysed 2 Sept 2025 Verify key 1DFNEGUKIPXV 99.82% Batch 50-502 BPC-157 10 mg Method HPLC + MS Analysed 27 Jun 2025 Verify key 35UHTDRKAUD9 99.72% Batch aura004 Retatrutide 30 mg (RT-30) Method HPLC + MS Analysed 28 Jul 2025 Verify key 1TYDHB4ZY3TG TB-500 12.58 mg BPC-157 13.02 mg GHK-Cu 57.12 mg KPV 10.77 mg Batch 50-502 KLOW 80 Blend (TB-500 / BPC-157 / GHK-Cu / KPV) Method HPLC + MS Analysed 19 Jun 2025 Verify key ZIDKJ1BNH944 99.53% Batch 50-502 Semax 10 mg Method HPLC + MS Analysed 27 Jun 2025 Verify key SBMIHKY77A3D 99.88% Batch aura003 Tirzepatide 15 mg Method HPLC + MS Analysed 10 Jul 2025 Verify key RLBA86SNPV7B 11.15 mg 10.95 mg (99.678% / 99.675%) Batch green Selank 10 mg Method HPLC + MS Analysed 22 Dec 2025 Verify key AI6GEKBHTVLE 21.00 mg 19.45 mg (99.733% / 99.740%) Batch LOT#0709 Tirzepatide 20 mg Method HPLC + MS Analysed 23 Sept 2025 Verify key 9C8B948J3P1E 66.93 mg 66.41 mg (99.951% / 99.865%) Batch LOT#0709 Retatrutide 60 mg Method HPLC + MS Analysed 23 Sept 2025 Verify key MB7FH4LCXYBM 50.28 mg 50.51 mg (99.868% / 99.856%) Batch 1029 Tirzepatide 50 mg Method HPLC + MS Analysed 25 Nov 2025 Verify key NF8JR6KHSPBX 99.45% Batch aura004 MOTS-c 40 mg Method HPLC + MS Analysed 28 Jul 2025 Verify key T187RFET9A79 5.70 mg / 17.1 IU 5.33 mg / 15.99 IU (97.793% / 97.788%) Batch black HGH 15 IU (rHGH) Method HPLC + MS Analysed 22 Dec 2025 Verify key CIUIKFEVAMSK 41.47 mg 41.93 mg (99.839% / 99.817%) Batch 1029 Tirzepatide 40 mg Method HPLC + MS Analysed 25 Nov 2025 Verify key 3ADW9BYCRVPD CJC-1295 5.11 mg Ipamorelin 5.39 mg Batch aura004 CJC-1295 no DAC / Ipamorelin 10 mg Blend Method HPLC + MS Analysed 28 Jul 2025 Verify key A8WIEFR2GQTU 11.56 mg Batch 50-502 Selank 10 mg Method HPLC + MS Analysed 17 Jun 2025 Verify key Q7RL2RT7WBLI 10.57 mg Batch aura003 SNAP-8 10 mg Method HPLC + MS Analysed 10 Jul 2025 Verify key HAEY4SQVXUFJ 31.74 mg Batch aura003 Tirzepatide 30 mg Method HPLC + MS Analysed 10 Jul 2025 Verify key MEZVVEBVFPHX 22.77 mg (99.497%) Batch 50-502 Retatrutide 20 mg Method HPLC + MS Analysed 27 Jun 2025 Verify key UQIBJDDE5RU5 TB-500 11.58 mg BPC-157 12.02 mg GHK-Cu 58.51 mg Batch 50-502 Glow70 (TB-500 / BPC-157 / GHK-Cu) Blend Method HPLC + MS Analysed 19 Jun 2025 Verify key CRSDQ7BI7J2X 559.21 mg 563.14 mg Batch 1028 NAD+ 500 mg Method HPLC + MS Analysed 25 Nov 2025 Verify key ZBG687STZYM8 16.15 mg (99.675%) Batch 50-502 Ipamorelin 10 mg Method HPLC + MS Analysed 17 Jun 2025 Verify key 6X5JEFUWW2WA GHK-Cu 62.95 mg BPC-157 11.24 mg TB-500 10.91 mg Batch GLOW-2026-01 Glow70 (TB-500 / BPC-157 / GHK-Cu) Blend Method HPLC + MS Analysed 2 Feb 2026 Verify key LPBBDE3F882W GHK-Cu 56.05 mg BPC-157 10.75 mg TB-500 10.73 mg KPV 10.65 mg Batch KLOW-2026-01 KLOW 80 Blend (TB-500 / BPC-157 / GHK-Cu / KPV) Method HPLC + MS Analysed 2 Feb 2026 Verify key GFVYTNJN6Z8G 67.47 mg (99.808%) Batch TIRZ-60-2025-12 Tirzepatide 60 mg Method HPLC + MS Analysed 9 Dec 2025 Verify key HFLYZVPU4WT6 10.42 mg (99.794%) Batch RETA-10-2026-01 Retatrutide 10 mg Method HPLC + MS Analysed 2 Feb 2026 Verify key USHTNKXVYDE7 GHK-Cu 68.01 mg BPC-157 12.57 mg TB-500 8.74 mg KPV 10.97 mg Batch LYKL/2025-07-18 KLOW 80 Blend (TB-500 / BPC-157 / GHK-Cu / KPV) Method HPLC + MS Analysed 15 Aug 2025 Verify key NDLPZQ4FDQ4M 10.79 mg (99.562%) Batch LIYU2025RT20250808 Retatrutide 10 mg Method HPLC + MS Analysed 26 Aug 2025 Verify key GJL7X7RAC6GQ 11.24 mg (99.833%) Batch LIYU20250901 Melanotan II 10 mg Method HPLC + MS Analysed 18 Sept 2025 Verify key NKR7ER8DYMZB 14.50 mg (99.863%) blind identification confirmed Batch Blind GLP-1 Panel Retatrutide (Blind Test) Method HPLC + MS Analysed 8 Apr 2026 Verify key 9FFPIESBX6RV 1.991 EU/vial within pharmacopoeial limits Batch Safety Panel Endotoxin Analysis (LAL) Method Immunoassay Analysed 9 Apr 2026 Verify key 15SIWA3Z8PGB As, Cd, Pb, Hg not detected Batch Safety Panel Heavy Metals (As / Cd / Pb / Hg) Method Mass Spectrometry Analysed 8 Apr 2026 Verify key 3BY6Y2IKXCJ6 99.81% Batch LIYU20250901 BPC-157 10 mg Method HPLC + MS Analysed 18 Sept 2025 Verify key 68QWVQASYIAR 99.04% Batch LIYU20250901 TB-500 10 mg Method HPLC + MS Analysed 18 Sept 2025 Verify key Y3S1I57GMTPV 99.86% Batch LIYUTR20250808 Tirzepatide 20 mg Method HPLC + MS Analysed 26 Aug 2025 Verify key U2ILVFLUQXNZ CJC-1295 5.26 mg Ipamorelin 4.95 mg (label-matched) Batch LIYU20250901 CJC-1295 no DAC 5 mg + Ipamorelin 5 mg Blend Method HPLC + MS Analysed 17 Sept 2025 Verify key PQ7ZDRCZ9UMS 99.83% Batch LIYU20250901 Ipamorelin 10 mg Method HPLC + MS Analysed 18 Sept 2025 Verify key 4K11FZZBIF63 99.74% Batch LIYU20250901 Tirzepatide 30 mg Method HPLC + MS Analysed 18 Sept 2025 Verify key DYQ9DMCNS1NR 99.63% Batch LYXA112025916 Semax 11 mg Method HPLC + MS Analysed 2 Oct 2025 Verify key 7LCUA7IEQ3TL BPC-157 9.23 mg TB-500 9.79 mg (label-matched) Batch LIYU20250901 BB20 (BPC-157 10 mg + TB-500 10 mg) Blend Method HPLC + MS Analysed 17 Sept 2025 Verify key Y8VVP1PH79CT 99.59% Batch LYSK112025916 Selank 11 mg Method HPLC + MS Analysed 2 Oct 2025 Verify key CJ5MN94S7YAA 97.04% Batch LIYU20250901 IGF-1 LR3 1 mg Method HPLC + MS Analysed 18 Sept 2025 Verify key CECGF8RXKHLU 5.67 mg (99.706%) Batch Unknown AOD-9604 5 mg Method HPLC + MS Analysed 12 May 2026 Verify key GFUKSN5W2GHE 10.42 mg (99.555%) Batch ML10/2025-05 Melanotan 2 (MT-2) 10 mg Method HPLC + MS Analysed 15 May 2025 Verify key P26TNUKFQ48C 4.42 mg (99.630%) Batch 5AD/2025-04 AOD-9604 5 mg Method HPLC + MS Analysed 16 Apr 2025 Verify key AHYRCEBSDEJ2 1.13 mg (99.282%) Batch IG1/2025-05 IGF-1 LR3 1 mg Method HPLC + MS Analysed 15 May 2025 Verify key PJ8SIALJ6TRG 9.38 mg (99.560%) Batch ET10/2025-05 Epithalon 10 mg Method HPLC + MS Analysed 15 May 2025 Verify key X3TS4MD47N63 10.56 mg (99.933%) Batch Unknown BPC-157 10 mg Method HPLC + MS Analysed 12 May 2026 Verify key LRJDQBNSMF8D 65.82 mg (99.889%) Batch Unknown Tirzepatide 60 mg Method HPLC + MS Analysed 12 May 2026 Verify key R5EDRGGY4UGC 9.91 mg (99.369%) Batch TSM10/2025-04 Tesamorelin 10 mg Method HPLC + MS Analysed 16 Apr 2025 Verify key Y4CSYRT9GRUL 55.41 mg (99.875%) Batch 040126R50Y Retatrutide 50 mg Method HPLC Analysed 26 Apr 2026 Verify key VIDA1T32ATAE 10.12 mg (99.807%) Batch WWB-0830 TB-500 (TB-4) 10 mg Method HPLC + MS Analysed 30 Aug 2024 Verify key CK4GWXZKZA14 10.35 mg (99.753%) Batch MS10/2025-05 MOTS-c 10 mg Method HPLC + MS Analysed 15 May 2025 Verify key D8SC1LWGFBUX 10.41 mg (99.760%) Batch Unknown PT-141 10 mg Method HPLC + MS Analysed 12 May 2026 Verify key XV7QQEP4YIPU Ipamorelin 5.06 mg CJC-1295 (mod GRF 1-29) 5.25 mg Batch Unknown CJC-1295 no DAC 5 mg + Ipamorelin 5 mg Blend Method HPLC + MS Analysed 13 May 2026 Verify key 7JJ7ZRKGIGPV 9.66 mg (99.915%) Batch Unknown Ipamorelin 10 mg Method HPLC + MS Analysed 13 May 2026 Verify key SDRU6GR9F174 10.46 mg (98.137%) Batch Unknown Tesamorelin 10 mg Method HPLC + MS Analysed 13 May 2026 Verify key 91L3RBS2CR8H 9.77 mg (99.781%) Batch Unknown CJC-1295 no DAC 10 mg Method HPLC + MS Analysed 13 May 2026 Verify key DW3FDAT9GUGV Testing in progress These compounds are currently at Janoshik Analytical / VidaLabs for independent HPLC + MS analysis

doi: 10.1136/annrheumdis-2022-222370 10 LinCMAIsaacsJDCoolesFAH