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Insert the needle at an angle so the solvent runs down the inner wall, not onto the powder

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The carbon, sulphur, nitrogen and oxygen contents of the sintered products were determined by combustion analysis using a carbon-sulfur elemental mass induction analyser (EMIA) (Horiba, Longjumeau, France) and an elemental mass gas analyser (EMGA) (Horiba, Longjumeau, France)

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